无水三氯化铝催化合成3-乙酰氨基-N,N-二丙酸甲酯基苯胺的研究

A Study on the Synthesis of 3-Acetyl Amino -N,N-Two Propionic Acid Methoxycarbonyls Aniline with Anhydrous Aluminum Chloride as Catalyst

报道了用无水AlCl3作催化剂在低温下将3-氨基乙酰苯胺和丙烯酸甲酯转化为3-乙酰氨基-N,N-二丙酸甲酯基苯胺的新方法,其产品收率达到90%,纯度高于94%。

A new method of synthesis of 3- acetyl amino - N, N- two propionic acid methoxycarbonyls aniline was reported by using anhydrous aluminum chloride, 3-amino-acetanilide, and methyl acrylate at lower temperate, the yield was over 90%, the purity was over 94%.