摘要
研究了合成Co3O4前驱体的几个影响因素。实验选用氯化钴作为原料,碳酸钠作沉淀剂,Co离子浓度为60~70g/L,氯化钴/碳酸钠(摩尔比)比值在0.60-0.70之间,加液方式选择将沉淀剂加入氯化钴液中,沉淀时pH值控制在9.0~9.6。实验表明,在上述条件下,可以获得较好的Co3O4前驱体。
Some factors which affected the synthesis of Co304 precursor were studied. Cobalt chloride was selected as raw material, sodium carbonate as precipitant, the concentration of cobalt ion was 60 -70 g/L, the ratio( mol ratio) of cobalt chloride and sodium carbonate was among 0.60 - 0.70, precipitant was added into cobalt chloride solution and pH value was controled among 9.0 - 9.6 during precipitation, better Co3O4 precursor can be obtained.
出处
《矿冶工程》
CAS
CSCD
北大核心
2009年第6期92-95,共4页
Mining and Metallurgical Engineering
基金
中南林业科技大学人才引进项目