摘要
采用水热法合成了Na5[B2P3O13](NBP)和BaA lBO3F2(BABF),确定了合成NBP的最佳反应条件,确立并分析了合成纯相BABF时反应物浓度的适宜配比及其对产物的影响。同时对合成的NBP和BABF进行了XRD、SEM及倍频效应等性质的表征。
Na5 [ B2P3O13 ] (NBP) and BaAlBO3F2(BABF) nonlinear optical crystals have been synthesized by hydrothermal method, the moderate reaction conditions have also been determined. The feasible initial charging ratio has been investigated in order to fabricate pure BABF. The as-synthesized NBP and BABF are characterized by XRD, SEM and second harmornie generation effect measurement, respectively.
出处
《人工晶体学报》
EI
CAS
CSCD
北大核心
2009年第6期1446-1449,共4页
Journal of Synthetic Crystals