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烟草中游离态烟碱的测定 被引量:6

Determination on Free Nicotine in Tobacco
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摘要 用有机溶剂萃取烟草中的游离态烟碱,考查溶剂、萃取方式、料液比、提取时间、提取温度和振荡速度等对游离烟碱得率的影响。结果表明,料液比为1:30时,三氯甲烷为萃取溶剂,在40℃条件下提取30 min,摇床转速为200 r/min时,提取效果最好。 The free nicotine in tobacco was extracted by organic solvent,and the effects of solvent,extraction method,solid-liquid ratio,extraction time,extraction temperature and shake speed on yield rate of free nicotine were studied.The results showed that the extraction effect was the best when solid-liquid ratio of 1:30 with chloroform as extraction solvent,extraction time of 30 min with extraction temperature of 40℃and rotation speed of 200 r/min.
出处 《安徽农业科学》 CAS 北大核心 2009年第36期17946-17947,17956,共3页 Journal of Anhui Agricultural Sciences
关键词 烟草 游离烟碱 得率 Tobacco Free nicotine Yield rate
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