Zn2SiO4：Mn的水热法制备

HYDROTHERMAL SYNTHESIS OF Mn- DOPED Zn2SiO4

利用简易水热法原位合成制备踟2n2SiO4：Mn绿色荧光体，主要原料为TEOS（Tetraethyl orthosilicate），Zn（CH3COO）2·2H2O，Mn（CH3COO）2·4H2O．通过控制反应条件，合成出了具有空心和微米花状结构的硅酸锌掺锰，利用XRD，TEM，SEM和荧光光谱仪对其进行表征，并对其反应机理进行解释．

Green emitting Mn -doped Zn2SiO4 nanopartieles were synthesized by a simple hydrothermal method, using TEOS（Tetraethyl orthosilicate）, Zn（ CH3COO） 2·2H20, Mn（ CH3COO） 2·4H2O. The rod - like and micro - flower structures of Zn2SiO4 ： Mn were fabricated by controlling the reaction conditions. The samples were characterized by X - ray diffraction （ XRD ）, transmission electron microscopy （ TEM ）, scanning electron microscopy （SEM） and fluorescence spectroscopy. The growth mechanism of Zn2 SiO4·Mn was also explained.