3Burton H S, Abraham E P. Isolation of antibiotics from a species of Cephalosporium.Cephalosporins P1, P2, P3, P4 and P5 [J].Biochemical Journal, ! 951,50 ( 2 ) : 168.
4中华人民共和国农业部第253号公告,动物食品中兽药最高残留限量[S].2002.
5Dasenaki M E, Bletsou A A, Koulis G A, et al. Qualitative Multiresidue Screening Method for 143 Veterinary Drugs and Pharmaceuticals in Milk and Fish Tissue Using Liquid Chromatography Quadrupole- Time- of- Flight Mass Spectrometry [J]. Journal of agricultural and food chemistry, 2015,63 (18): 4493 -4508.
6Storey J M, Clark S B, Johnson A S, et al. Analysis of sulfonamides, trimethoprim, fluoroquinolones, quinolones, triphenyhnethane dyes and methyltestosterone in fish and shrimp using liquid chromatography - mass spectrometry [J] . Journal of Chromatography B ,2014,972:38-47.
7Dorival- Garcia N, Junza A, Zafra- G6mez A, et al. Simultaneous determination of quinolone and fl-lactam residues in raw cow milk samples using ultrasound-assisted extraction and dispersive- SPE prior to UHPLC - MS/MS analysis [J] . Food Control, 2016,60 : 382- 393.
8Barker S A, Long A R, Short C R.Isolation of drug residues from tissues by solid phase dispersion[J]. Journal of Chromatography A, 1989,475 ( 2 ) :353-361.
9Karageorgou E G, Samanidou V F. Application of ultrasound -assisted matrix solid-phase dispersion extraction to the HPLCconfirmatory determination of cephalosporin residues in milk [J]. Journal of separation science,2010,33:2862-2871.
10Liu X, Yu Y, Zhao M, et al. Solid phase extraction using magnetic core mesoporous shell microspheres with C18-modified interior pore-walls for residue analysis of cephalosporins in milk by LC-MS/MS [J] .Food chemistry ,2014,150:206-212.