摘要
采用微波辐射加热法,以壳寡糖为原料,设计并合成了一系列壳寡糖希夫碱的金属配合物,其结构经紫外吸收、红外光谱、元素分析、ICP光谱和热重分析确认。该法具有反应时间短、温度条件易控、操作简便等特点,是一个值得推广的绿色合成方法。
A series of chitooligosaccharides Schiff base complexes were synthesized from chitooligosaccharides under microwave irradiation and their structures were characterized by UV,IR,element analysis,ICP spectroscopy and TG.This method has advantages such as short time,easy operation and environmentally benign procedures compared with traditional method.
出处
《光谱实验室》
CAS
CSCD
北大核心
2010年第3期867-871,共5页
Chinese Journal of Spectroscopy Laboratory
基金
国家烟草专卖局重大科技攻关项目(110200401004)
关键词
壳寡糖
希夫碱
微波合成
结构表征
Chitooligosaccharides
Schiff Base
Microwave Synthesis
Characterization