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微波消解ICP-MS定量测定人体血清中14种微量元素 被引量:2

Simultaneous Determination of 14 Elements in Human Serum by ICP-MS with Microwave Digestion
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摘要 采用电感耦合等离子体-质谱法测定慢性肾炎患者及健康人血清中的Na、Mg、Al、K、Ca、Cr、Mn、Fe、Ni、Cu、Zn、As、Se和Pb等14种元素,以In作为内标进行基体效应的补偿,该方法快速灵敏,回收率为91.08%—l08.0%,相对标准偏差小于5.0%,结果令人满意,可应用于临床慢性肾炎患者血清中多种微量元素的同时检测。 The 14 kinds of trace element,Na,Mg,Al,K,Ca,Cr,Mn,Fe,Ni,Cu,Zn,As,Se and Pb in serum of chronic glomerulonephritis and health person were simultaneously determined by ICP-MS.In was as the internal standard to compensate the matrix effect.The recoveries are in the range of 91.08%—l08.0% with the relative standard deviations of less than 5.0%.The validated method for determining trace elements is simple,fast,which can be employed to the determination of trace elements in serum of chronic glomerulonephritis.
出处 《光谱实验室》 CAS CSCD 北大核心 2010年第3期1128-1131,共4页 Chinese Journal of Spectroscopy Laboratory
基金 辽宁省自然科学基金项目资助(No.20072073)
关键词 电感耦合等离子体-质谱法 慢性肾炎 血清 微量元素 ICP-MS Chronic Glomerulonephritis Serum Trace Elements
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