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球形SnO_2微晶水热法制备与表征 被引量：2

Hydrothermal Synthesis and Characterization of Spherical SnO_2 Microcrystals
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摘要 采用SnCl4.5H2O为原料,NaOH作沉淀剂,通过一个简单的水热过程制得球形SnO2微晶。样品的XRD和TEM表征结果表明反应温度、水热时间、不同的碱源和软模板对产物的形貌和尺度有一定的影响,球形SnO2微晶的形成机理可能是一个水热过程中的自组装行为。 The spherical SnO2 crystals with micrometer scale were synthesized by a simple hydrothermal process with SnCl4 · 5H2O as the starting materials and NaOH as the precipitant. The characterization results of XRD and TEM indicated that the morphologies and sizes of samples were influenced by hydrothermal temperature, hydrothermal time, different alkali and soft template. The possible growth mechanism of spherical structures is a self- assembly action during hydrothermal process.
作者 李子荣 郑胜彪 王军锋
机构地区 安徽科技学院理学院
出处 《安徽科技学院学报》 2010年第2期48-51,共4页 Journal of Anhui Science and Technology University
基金 安徽科技学院稳定人才项目(ZRC2007118) 安徽科技学院重点建设课程项目(zdkc0918)
关键词 水热 制备 表征 二氧化锡 Hydrothermal Synthesis Characterization Tin dioxide
分类号 O611.4 [理学—无机化学]
  • 相关文献

参考文献14

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二级参考文献12

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共引文献5

同被引文献23

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引证文献2

二级引证文献5

安徽科技学院学报
2010年 第2期

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