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中温烧结0.6Mg_4Nb_2O_9-0.4SrTiO_3复相陶瓷 被引量：3

The middle-temperature sintering of 0.6Mg_4Nb_2O_9-0.4SrTiO_3 composite ceramics
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摘要 采用传统固态反应方法制备0.6Mg4Nb2O9-0.4SrTiO3复合陶瓷。研究LiF掺杂对其烧结特性、相结构和微观形貌的的影响。通过X射线衍射(XRD)和扫面电镜(SEM)观察样品的相组成和显微结构。实验结果表明:1.5 wt%LiF添加,可将Mg4Nb2O9/SrTiO3陶瓷的致密化烧结温度从1300℃降至1100℃;XRD表明除主相Mg4Nb2O9、SrTiO3外,还有少量新相Sr(Ti1-xNbx)O3+δ生成。 The 0.6Mg4Nb2O9-0.4SrTiO3 composite ceramics was prepared by conventional solid-state reaction method.The effects of LiF addtion on the sintering behavior,phase compositions and microstructure of 0.6Mg4Nb2O9-0.4SrTiO3 specimen were studied.The samples were analyzed using X-ray diffraction and scanning electron microscopy techniques.The densification sintering temperature of 0.6Mg4Nb2O9＋0.4SrTiO3 is significantly lowed from 1300℃ to 1175℃ with 1.5 wt% LIF addtion.The main phases of Mg4Nb2O9 and SrTiO3 combined with small amount of Sr（Ti1-xNbx）O3＋δ were detected by XRD.
作者 裴翠锦 姚国光 田秀劳
机构地区 运城学院应用化学系 西安邮电学院理学院
出处 《西安邮电学院学报》 2010年第3期119-121,127,共4页 Journal of Xi'an Institute of Posts and Telecommunications
基金 陕西省自然科学基金资助项目(2009JM601)
关键词 复合陶瓷 X射线衍射 扫描电镜 LiF掺杂 composite ceramics XRD SEM LiF-doped
分类号 TM534 [电气工程—电器]
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参考文献14

  • 1Huang C L,Chen J Y.High-Q Microwave Dieleetries in the(Mg1-xCox)2TiO4 Ceramics[J].J.Am.Ceram.Soc,2009,92(2):379-383.
  • 2Prabhakaran S A,Mailadil T S.Microwave Dideetric Properties and Low-Temperature Sintering of Cerium Ox-ide for LTCC Applications[J].J.Am.Ceram.Soc,2009,92(1):96-104.
  • 3Zhang Q L,Yang H,Sun H P.A new microwave ce-ramic with low-permittivity for LTCC applications[J].J.Fur.Ceram.Soe,2008,28(3):605-608.
  • 4Akinori K,Hirotaka O.Low-temperature sintering and microstructure of Mg4(NB2-x.Vx)09 microwave dieleetric xeramic by V substitution for Nb[J].Jpn.J.Appl.Phys,2003,42(1):6154-6157.
  • 5Dai S X,Huang R F,Wiloox D L.Use of titanates to achieve a temperature-stable low-temperature co-fired ce-ramic dideetric for wireless applications[J].J.Am.Cer-am.Soc,2002,85(4):828-832.
  • 6Ogawa H,Karl A,Ishihara S.Crystal Structure of Corundum Type Mg4(Nb2-xTax)09 Microwave Dielec-tric Ceramics with Low Dielectric Loss[J].J.Eur.Cer-am.Soc,2003,23(14):2485-2488.
  • 7Kan A.,Ogawa H,Yokoi A.Sintering Temperature Dependence of Miciowsve Dielectric Properties in Mg4 (TaNb1-xVx)09 Compounas[J].Mater.Res.Bull,2006,41(6):1178-1184.
  • 8Kan A,Ogawa H,Yokoi A.Crystal Structural Refine-mealt of Corundum-Structured A4M2O9(A=Co and Mg,M=Nb and Ta)Microwave Dideetric Ceramics by High-Temperature X-ray Powder Diffraction[J].J.Eur.Ceram.Soc,2007,27(8):2977-2981.
  • 9Liu P,Su W A,Yao G G.The Sintering Behavior and Microwave Dielectric Properties of Mg4(Nb,Sb)O9 Ce-ramics[J].J.Electroceram,2008,21(1-4):478-482.
  • 10Lim SW,Bang JJ.Microwave dielectric properties of Mg4Nb2O3 ceramics produced by hydrothermal synthesis[J].J.Electroeram,2009,23(2-4):116-120.

同被引文献21

  • 1徐甲强,贾晓华,娄向东,李超.低温固相反应合成Zn_2SnO_4及其气敏性能[J].硅酸盐学报,2006,34(3):303-307. 被引量：17
  • 2徐甲强,张海林,潘庆谊,向群,李超.水热合成工艺对Zn_2SnO_4纳米晶形貌及电化学性能的影响(英文)[J].硅酸盐学报,2007,35(8):978-981. 被引量：6
  • 3D. E. Saife. Oxide semiconductors in photoelect rochemical conversion of solar energy[J]. Solar Energy, 1982, 25(1):41-54.
  • 4A. Fang, A. H. Huang. Hydrothermal preparation and characterization of Zn2SnO4 particles [ J ]. Mater. Res. Bull., 2001, 36(7): 1391-1397.
  • 5A. Petsom, S. Roengsumran et al. An oxygen index evaluation of flammability for zinc hydroxystannate and zinc stannate as synergistic flame retardants for acrylonit rile-butadiene-styrene copolymer[J ]. Polym Degradation Stab, 2003, 80(1) :17-22.
  • 6X. J. Zhua, L. M. Genga, F. Q. Zhangb, etal. Synthesis and performance of Zn2SnO4 as anode materials for lithium ionbatteries by hydrothermal method[J]. Journal of Power Sources, 2009,189 (1) : 828-831.
  • 7Cun Wang and Bo-Qing Xu. Coprecipitation synthesis and optical absorption property of ZnzTixSn1- xO4 (0≤x≤1) solid solutions[J ]. Journal of Materials Science, 2009,44 (3) :919-925.
  • 8Liu Xiaobin, Zhou Huanfu, Fang Liang. Phase struc- ture and microwave dielectric properties of (1 --x) LizZrTi4Olz-xTiOz ceramics[J]. J Alloys Compd, 2012, 515(25): 22-25.
  • 9Lei Wei, Lu Wenzhong. Temperature compensating ZnA12 O4-Co2 TiO4 spinel-based lowpermittivity micro- wave dielectric ceramics[J]. Ceram Int, 2012, 38(1) : 99-103.
  • 10Kim D W, Kim J R, Yoon S K. Microwave Dielectric Properties of Low-Fired 13NbOs [J]. J Am Ceram Soc, 2002, 85(11): 2759-2762.

引证文献3

二级引证文献9

西安邮电学院学报
2010年 第3期

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