摘要
主要研究了几种不同制取方法和不同因素对固体酸CsH2PO4的影响,并用X-射线衍射仪(日本理学)分析表征其结构,得出制备酸CsH2PO4的最佳条件和方法是:选择在70℃恒温,Cs+浓度为15.4mol.L-1,pH=7的反应条件下甲醇萃取。
The effcet of different preparation methods and different reaction conditions on crystal form of polycrystalline power CsH2PO4 are studied.The crystal structure are analyed by X-ray diffraction(Rigaku,JAPAN).The best condition is as follows:70℃ isothermal reaction,the concentration of Cs+ is 15.4mol·L-1,acidity control pH=7 and methanol is selected as extraction agent.
出处
《安阳师范学院学报》
2010年第2期72-76,共5页
Journal of Anyang Normal University