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吡氟草胺原药毛细管气相色谱分析 被引量:4

A Quantitative Analysis of Diflufenican TC by Capillary Gas Chromatography
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摘要 采用气相色谱仪、HP-5毛细管色谱柱、氢火焰离子化检测器(FID),对除草剂吡氟草胺原药样品进行定量分析。结果表明:吡氟草胺浓度为0.41~51.5μg/mL范围内,方法线性相关系数为0.99998,精密度实验的相对标准偏差为0.14%,平均回收率为99.74%。 A quantitative gas chromatographic method adopting FID and HP-5 capillary column has been developed for the determination of the diflufenican TC.The assay exhibited a good linearity in diflufenican concentration range from 0.41 to 51.5 μg /mL,with correlation coefficient of 0.999 98.The variation coefficient and average recovery were 0.14% and 99.74%,respectively.
出处 《精细化工中间体》 CAS 2010年第3期70-72,共3页 Fine Chemical Intermediates
基金 贵州省农业科技攻关资助项目(No.20083053)
关键词 吡氟草胺 除草剂 毛细管气相色谱法 diflufenican herbicide capillary gas chromatography
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参考文献5

  • 1刘长令.世界农药大全[M].北京:化学工业出版社,2002..
  • 2高静,马忠国.吡氟草胺的高效液相色谱分析[J].化学工程师,2005,19(12):22-23. 被引量:5
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二级参考文献1

  • 1Cramp Michael Colin; Gilmour James; Parnell Edgar William,New herbicidal nicotinamide derivatives.EP0053011 ,1982.

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