摘要
以水杨醛为原料,经碘代反应合成了3-碘水杨醛,并在微波辅助作用下与醋酸铜作用合成3-碘水杨醛合铜配合物。此法操作简便,绿色环保。
3 -iodo- salicylaldehyde was synthesized by salicylaldehyde and iodine in acetum. A new complex, 3 - iodo - salicylalidene - copper ( Ⅱ) was designed and synthesized by solid - phase reaction under microwave irradiation. The procedure of the synthesis simple and environ mental.
出处
《宿州学院学报》
2010年第5期18-19,共2页
Journal of Suzhou University
基金
江苏省高校自然科学基金(09KJD150005)
徐州师范大学本科学生科研课题(xskt2010073)
关键词
微波固相合成
3-碘水杨醛
3-碘水杨醛合铜
microwave solid - phase synthesis
3 - iodo - salicylaldehyde
3 - iodo - salicylalidcne - copper(Ⅱ)