期刊文献+

微波固相法合成3-碘水杨醛合铜 被引量:1

Microwave Solid-phase Synthesis of 3-Iodo-Salicylalidene-Copper(Ⅱ)
下载PDF
导出
摘要 以水杨醛为原料,经碘代反应合成了3-碘水杨醛,并在微波辅助作用下与醋酸铜作用合成3-碘水杨醛合铜配合物。此法操作简便,绿色环保。 3 -iodo- salicylaldehyde was synthesized by salicylaldehyde and iodine in acetum. A new complex, 3 - iodo - salicylalidene - copper ( Ⅱ) was designed and synthesized by solid - phase reaction under microwave irradiation. The procedure of the synthesis simple and environ mental.
出处 《宿州学院学报》 2010年第5期18-19,共2页 Journal of Suzhou University
基金 江苏省高校自然科学基金(09KJD150005) 徐州师范大学本科学生科研课题(xskt2010073)
关键词 微波固相合成 3-碘水杨醛 3-碘水杨醛合铜 microwave solid - phase synthesis 3 - iodo - salicylaldehyde 3 - iodo - salicylalidcne - copper(Ⅱ)
  • 引文网络
  • 相关文献

参考文献3

二级参考文献39

  • 1张蕊,牛雪平,赵文岩,李焕珠.3,5-二碘代水杨醛-芳胺Schiff碱的合成与生物活性测试[J].内蒙古大学学报(自然科学版),2004,35(5):557-561. 被引量:6
  • 2黄秋亚,朱槿,邓金根.金属催化硫醚的不对称氧化研究进展[J].有机化学,2005,25(5):496-506. 被引量:11
  • 3Kornyushyna, O.; Stemmler, A. J.; Graybosch, D. M.; Bergenthal, I.; Burrows, C. J. Bioconjugate Chem. 2005, 16, 178--183.
  • 4Nielsen, M.; Dauksaite, V.; Kjems, J.; Gothelf, K. V. Bioconjugate Chem. 2005, 16, 981-985.
  • 5Xiang, Y.; Tong, A.; Jin, P.; Ju, Y. Ong. Lett. 2006, 8, 2863-2866.
  • 6Cruces Blanco, C.; Garcia Sanchez, E Anal. Chem. 1984, 56, 2035-2038.
  • 7Tanaka, M.; Imai, M.; Yamamoto, Y.; Tanaka, K.; Shimowatari, M.; Nagumo, S.; Kawahara, N.; Suemune, H. Org. Lett. 2003, 5, 1365-1367.
  • 8Bajwa, N.; Jennings, M. R J. Org. Chem. 2006, 71, 3646-3649.
  • 9Cao, P.; Fang, R. Q.; Li, H. Q.; Zhu, H. L. Chinese J. Struct. Chem. 2007, 11, 1320-1324.
  • 10Zhang, L. N.; Shi, L.; Fang, R. Q.; Zhu, H. L. Chinese J. Struct. Chem. 2008, 2, 200-204.

共引文献19

同被引文献16

  • 1梁学军,徐锁平.碘代水杨醛合成的新方法[J].宿州学院学报,2008,23(5):115-116. 被引量:15
  • 2张蕊,牛雪平,赵文岩,李焕珠.3,5-二碘代水杨醛-芳胺Schiff碱的合成与生物活性测试[J].内蒙古大学学报(自然科学版),2004,35(5):557-561. 被引量:6
  • 3疏翠.藤黄微球菌过氧化氢酶发酵条件优化、诱变育种及其基因的克隆、表达纯化[D].上海:东华大学,2010.
  • 4Nielsen M, Dauksaite V, Kjems J, et al. DNA - directed coupling of organic modules by multiple parallel reductive aminations and subsequent cleavage of selected DNA sequences [ J ]. Bioconjugate Chemistry, 2005,1 6 (4) : 981 - 985.
  • 5Blanco C C, Sfinchez F G. Speetmfluorlmetrle and synchronous scanning first derivative spectrofluorimetry for determination of magnesium with salieylaldehyde2 - pyridylhydrazone [ J ]. Analytical Chemistry, 1984, 56 (12) :2035 -2038.
  • 6Xiao Z P, Fang R Q, Shi L, et al. Synthesis, crystal structure, and growth inhibition of human hepatoma cell (HepG2) of polyphenolic compounds based on gallates [J]. Canadian Journal of Chemistry,2007,85 (11) :951- 957.
  • 7Averseng F, Lacroix P G, Malfant I, et al. Enhanced second harmonic generation on passing from a mono to a dicopper (II) bis - (salicylaldiminato) Schiff base comple[J]. Inor- ganic Chemistry,2001,40 ( 15 ) : 3797 - 3804.
  • 8David C, Daniel G. Synthesis of a 4, 6 - disubstituted diberrr, ofuran 13 - sheet initiator by reduetive radical aryla- tion of benzene [ J ]. J Org Chem, 2005,70 (6) : 2384 - 2386.
  • 9杨明星,林深,张晓凤,陈丽娟.N-苯甲酰基水杨酰肼为配体的三核镍(Ⅱ)配合物的合成与结构[J].分子科学学报,2008,24(4):250-256. 被引量:2
  • 10徐锁平,裴元,徐郭,苏文信,束君仙.3,5-二碘水杨醛缩乙醇胺的晶体结构及抑菌活性[J].徐州师范大学学报(自然科学版),2010,28(2):57-60. 被引量:4

引证文献1

二级引证文献1

相关主题

;
使用帮助 返回顶部