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Application of Statistical Design Strategies to Optimize the Preparation of ZnO Nanoparticles by Hydrothermal Technique

Application of Statistical Design Strategies to Optimize the Preparation of ZnO Nanoparticles by Hydrothermal Technique
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摘要 Synthesis of ZnO nanoparticles by hydrothermal technique in presence of cetyltrimethylammonium bromide (CTAB) as surfactant was carried out by statistically designed experiments based on Box Behnken method. The mean parameters, surfactant concentration, time and temperature have been studied to show their effect on ZnO particle size and morphology. The results of experimental design indicate that the surfactant concentration, reaction time and temperature were significant. ZnO particles were investigated using XRD and SEM and the findings show that ZnO nanoparticles were formed at 100 ℃ and their crystallinity were improved with temperature rise from 100 to 200 ℃. Particle size of ZnO in the range of 39-76 nm is achieved using this technique.
作者 I.A. Mkhalid
机构地区 Chemistry Department
出处 《Journal of Environmental Science and Engineering》 2010年第6期67-72,共6页 环境科学与工程(英文版)
关键词 Statistical design ZnO NANOPARTICLES SURFACTANT hydrothermal. ZnO纳米粒子 统计方法 氧化锌 设计策略 十六烷基三甲基溴化铵 水热法 表面活性剂 制备
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参考文献13

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