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N,N-二甲基叠氮乙基胺合成研究 被引量：7

Study on Synthesis of 2-Azido-N,N-Dimethylethanamine
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摘要 对2条N,N-二甲基叠氮乙基胺(DMAZ)的合成路线进行了对比研究,制备出纯度>99%的DMAZ,产品经FT-IR、GC-MS、1H-NMR表征确认其正确结构。 A comparative study on two synthesis routes of 2-azido-N,N-dimethylethanamine（DMAZ） was carried out. The product DMAZ with the purity over 99% was prepared, and its right structure was confirmed by FT-IR, GC-MS, 1H- NMR.
作者 池俊杰 王建伟 王文浩 常伟林 张晓勤 曲贵晨
机构地区 黎明化工研究院
出处 《化学推进剂与高分子材料》 CAS 2010年第4期39-41,共3页 Chemical Propellants & Polymeric Materials
关键词 DMAZ 液体燃料 叠氮化合物 合成 DMAZ liquid fuel azide synthesis
分类号 V512 [航空宇航科学与技术—航空宇航推进理论与工程]
  • 相关文献

参考文献7

  • 1Thompson Darren M. Tertiary amine azides in liquid or gel fuels in gas generator systems: US, 6210504 [P]. 2001.
  • 2Thompson Darren M. Amine azides used as monopropellants: US, 6299654[P]. 2001.
  • 3Thompson Darren M. Tertiary amine azides in hypergolic liquid or gel fuels propellant systems: US, 6013143[P].2000.
  • 4Barrie Mellor. A preliminary technical review of DMAZ: A low-toxicity hypergolic fuel[C]//Proc 2nd Int Conference on Green Propellants for Space Propulsion. Cagliari, Sardinia, ESA SP-557, 2004.
  • 5John Weijlasrd, Max Tishler. Quaternary ammonium ethyl thiolcarbamates: US, 2642428[P]. 1953.
  • 6Paul D Bartlett, Sidney D Ross, Swain C Gardner. Kinetics and mechanism of the reactions of tertiary β-chloroethylamines in solution, Ⅲ.β-chloroethyldiethylamine and tris-β-chloroethylamine[R]. Havard University, 1949.
  • 7Aziza Benalil, Bertrand Carboni, Michel Vaultier. Synthesis of 1,2-aminoaziders conversion to unsymmetrical vicinal diamines by catalytic hydrogenation or reductive alkylation with dichloroboranes [J]. Tetrahedron, 1991, 47(28): 8 177-8 194.

同被引文献64

  • 1符全军.液体推进剂的现状及未来发展趋势[J].火箭推进,2004,30(1):1-6. 被引量：18
  • 2贺芳,方涛,李亚裕,米镇涛.新型绿色液体推进剂研究进展[J].火炸药学报,2006,29(4):54-57. 被引量：35
  • 3Aziza Benalil, Bertrand Carbonil, Michel Vautier. Synthesis of 1,2-aminoazide[J]. Tetrahedron, 1991, 47(38): 8 177-8 194.
  • 4Barrie Mellor. A preliminary technical review of DMAZ: a low-toxicity hypergolic fuel[C]//Proc 2nd Int Conference on Green Propellants for Space Propulsion. Cagliari, Sardinia, ESA SP - 557, 2004.
  • 5Mach I, Incmach I. Pioneer in nano-structure, advanced materials and aerospace[EB/OL]. [2004 - 08 - 05]. http://www.machichemicals.com.
  • 6Frankel Milton B, Wilson Edgar R. Tris(2-azidoethyl) amine and method of preparation thereof: US, 4499723[P]. 1985.
  • 7Richman K W, Griffith K N, Liotta C L, et al. Novel beta-substituted ethylazide derivatives as potential new liquid propellant fuels[C]//JANNAF54 Propulsion Meeting. American Pacific Corporation and Georgia Institute of Technology Atlanta 2007.
  • 8Thompson Darren M. Tertiary amine azides in liquid or gel fuels in gas generator systems: US, 6210504[J]. 2001.
  • 9Thompson Darren M. Amine azides used as monopropellants: US, 6299654[P]. 2001.
  • 10Thompson Darren M. Tertiary amine azides in hypergolic liquid or gel fuels propellant systems: US, 6013143[P]. 2000.

引证文献7

二级引证文献15

化学推进剂与高分子材料
2010年 第4期

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