摘要
DMA-LiCl-cellulose is coated on 3-aminopropyl silica gel as chiral stationary phases for high performance liquid chromatography(HPLC),and its chiral column(250 mm×2.0mm,i.d.)was prepared under the pressure of 40 MPa.In the normal phase of high performance liquid chromatography,21 chiral compounds,including alcohols,acids,amines,amino acids and drugs,were resolved on this column,13 kinds of chiral compounds have been separated.The results indicate that the chiral stationary phase possesses a good chiral separation ability.
DMA-LiCl-cellulose is coated on 3-aminopropyl silica gel as chiral stationary phases for high performance liquid chromatography（HPLC）,and its chiral column（250 mm×2.0mm,i.d.）was prepared under the pressure of 40 MPa.In the normal phase of high performance liquid chromatography,21 chiral compounds,including alcohols,acids,amines,amino acids and drugs,were resolved on this column,13 kinds of chiral compounds have been separated.The results indicate that the chiral stationary phase possesses a good chiral separation ability.
出处
《化学研究与应用》
CAS
CSCD
北大核心
2010年第7期907-910,共4页
Chemical Research and Application
基金
国家自然科学基金项目(20775066)
云南省自然科学基金重点项目(2005E0006Z)
关键词
非衍生纤维素
高效液相色谱
手性固定相
手性化合物
手性拆分
DMA-LiCl-cellulose
high-performance liquid chromatography
chiral stationary phase
chiral compounds
chiral separation
