微乳体系相图及超微CuI晶体的合成与研究

Microemulsion System Phase Diagram and Synthesis and Study of Micro-CuI Crystal

考察了W([H2O]/[SDS])、T(温度)对SDS/正丁醇/环己烷/水四元微乳液体系相图的影响,并在T=60℃时利用此体系合成了超微的碘化亚铜晶体。用XRD、IR、TEM对产物进行了表征。结果表明:当W([H2O]/[SDS])=20、T=60℃时所得到的碘化亚铜晶体是粒径在100nm左右的块状立方晶体。

The influence of W（ / ）,T（temperature） on the SDS /n-butanol / cyclohexane / water quaternary microemulsion phase diagrams was studied.And,this system was used tosynthesiz the cubic CuI crystal when the temperature is 60℃.Via XRD,IR,TEM,EDS,the result shows： When W（ / ） =20、T=60℃ gained CuI and size is about 100nm of cubic crystals.