摘要
以L-苯丙氨酸为原料,经还原和关环反应合成了(S)-4-苄基-2-噁唑烷酮,总收率66%,其结构经1HNMR,13C NMR和HR-MS表征。
(S)-4-benzyl-2-oxazolidinone in total yield of 66% was synthesized by the reaction of reduction and ring-closing from L-phenylalanine.The structure was characterized by 1H NMR,13C NMR and HR-MS.
出处
《合成化学》
CAS
CSCD
北大核心
2010年第4期490-492,共3页
Chinese Journal of Synthetic Chemistry
基金
上海市科委科研计划资助项目(07DZ19503-2)
关键词
L-苯丙氨酸
噁唑烷酮
合成
工艺改进
L-phenylalanine
oxazolidinone
synthesis
process improvement