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固相微萃取/气相色谱/质谱法分析锦鸡儿茎挥发性成分 被引量:12

Volatile Oils in Stem of Caragana sinica by Head-pace Solid Micro-extraction
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摘要 目的:研究锦鸡儿挥发性成分。方法:首次采用固相微萃取/气相色谱/质谱法(HS-SPME-GC-MS)分析锦鸡儿茎中挥发油化学成分。结果:共鉴定出19个成分,占总挥发油成分峰面积的99.98%。结论:主要为烯烃(55.79%)和饱和烷烃类化合物(22.99%)。Z-5-十九碳烯(31.65%),8-十七碳烯(15.82%),二十八烷(9.48%),十七烷(7.66%),二十二烷(5.85%),6,9-十七碳二烯(5.15%)和十九烷(5.02%)是锦鸡儿茎的主要挥发性成分。 Objective:To study the volatiles of Caragana sinica. Method:The volatiles were analyzed by head-space solid micro-extraction,coupled with GC-MS for the first time. Result:Ninteen compounds were identified from the C. sinicaand account for 99. 98% of the total volatiles. Conclusion:Olefin ( 55. 79% ) and alkane (22. 99% ) were dominant volatiles. Z-5-nonadecene(31. 65% ),8-heptadecene(15. 82% ),octacosane(9. 48% ),heptadecane(7. 66% ),docosane ( 5. 85% ),6,9-heptadecadiene ( 5. 15% ) and nonadecane ( 5. 02% ) were the main compounds.
出处 《中国实验方剂学杂志》 CAS 北大核心 2010年第10期63-64,共2页 Chinese Journal of Experimental Traditional Medical Formulae
基金 河南省骨干教师资助计划(2008-755)
关键词 锦鸡儿 挥发油 固相微萃取/气相色谱/质谱法 Caragana sinica volatiles HS-SPME-GC-MS
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