期刊文献+

广谱高效蚊虫驱避剂DEET的合成 被引量:1

下载PDF
导出
摘要 应用Schotten-Baumann反应原理,选用SoCl_2作为酰氯化试剂,完成了酰胺化反应物的制备,其收率达到85%,用气相色谱测定,含量达95%。
作者 闫盛
出处 《石油化工应用》 CAS 2010年第8期16-17,共2页 Petrochemical Industry Application
  • 相关文献

参考文献4

二级参考文献5

  • 1蔡照胜,化学世界,1994年,1期,17页
  • 2章思规,精细有机化学品技术手册,1991年,581页
  • 3施达常,医药工业,1985年,16卷,3期,42页
  • 4陈再谋.驱虫剂[J]日用化学工业,1986(02).
  • 5[美]米勒等 著,董庭威等.现代有机化学实验[M]上海翻译出版社,1987.

共引文献8

同被引文献10

  • 1HELLESTAD V J, WITTHUHN B A, FALLON A M. The Insect Repellent DEET (N,N-Diethyl-3-methyl-benzamide) Increases the Synthesis ofGlutathione S-transferase in Cultured Mosquito Cells[J]. Cell Biology and Toxicology, 2011, 27: 149-157.
  • 2BHATTACFIARYA A, PLATA R E, VILLARREAL V, et ol. An Efficient Conversion of Nitriles to Amides: Application in the Synthesis of N,fl-Diethyl-meta-toluamide (DEET)[J]. Tetrahedron Letters, 2006, 47(4): 505-506.
  • 3HU Mei, HU Jiang-lir: SE Xiao, et oL Palladium-1, 10-phenanthroline Complex Encaged in Y Zeolite: An Efficient and Highly Recyclable Heterogeneous Catalyst for Aminocarbonylation [J]. Applied Catalysis A: General, 2014, 475: 40-47.
  • 4MATTHIAS K, ROMAN M. Continuous Production of Aromatic Carboxylic Acid Amides: WO, 2011000459[P]. 2011-01-06.
  • 5朱益民,张越.固定床一步合成MⅣ一二乙基间甲基苯甲酰胺的方法:CN,101362707[P].2009-02-11.
  • 6ZHUANG Zhe, HU Zhi-ping, LIAO Wei-wei. Asymmetric Synthesis of Functionalized Dihydronaphthoquinones Containing Quaternary Carbon Centers via a Metal-free Catalytic Intramolecular Acylcyanation of Activated Alkenes [J]. Organic Letters, 2014, 16(12): 3380-3383.
  • 7CRISENZA G E M, MCREANOR N G, BOWER J F. Branch- selective, Iridium-catalyzed Hydroarylation of Monosubstituted Alkenes via a Cooperative Destabilization Strategy [J]. Journal of the American Chemical Society, 2014, 136(29): 10258-10261.
  • 8HABECK J C, DIOP L, DICKMAN M. Synthesis of N, N-Diethyl-3-methylbenzamide (DEET): Two Ways to the Same Goal[J]. Journal of Chemical Education, 2010, 87(5): 528-529.
  • 9KHALAFI-NEZHAD A, PARHAMI A, SOLTANI R, et ol. Efficient Method for the Direct Preparation of Amides from Carboxylic Acids Using Tosyl Chloride under Solvent-flee Conditions[J]. Tetrahedron Letters, 2005, 46(40): 6879-6882.
  • 10RAO A N, GANESAN K, VIJAYARGHAVAN R. Process for the Preparation ofN, N-Disubstitnted Carboxamide: WO, 2013065059[P]. 2013-05-10.

引证文献1

二级引证文献1

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部