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介孔有机-无机杂化材料NH_2-MCM-41的合成与表征 被引量：1

Synthesis and characterization of organic-inorganic hybrid NH_2-MCM-41
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摘要 以正硅酸乙酯为硅源,十六烷基三甲基溴化铵为模板剂,合成介孔硅基材料MCM-41.通过有机硅烷偶连法将3-氨丙基三乙氧基硅烷嫁接到介孔材料MCM-41上,得到氨基官能化的介孔材料NH2-MCM-41.利用XRD、FT-IR、N2吸附-脱附和ICP对合成的杂化材料进行表征. Periodic Mesoporous Organosilicas MCM-41 is synthesized by taking TEOS as silica source and CBTA as template agent.The coupling agent 3-aminopropyl triethoxysilane is introduced into the inorganic mesoporous materials MCM-41,so the amino-functionalized mesoporous material NH2-MCM-41 is obtained.The hybrid material is characterized by means of X-ray diffraction,FT-IR,N2 adsorption-desorption experiments and elemental analysis.
作者 高文秀 王景峰 杨艳艳
机构地区 吉林化工学院化学与制药工程学院
出处 《吉林化工学院学报》 CAS 2010年第4期21-23,共3页 Journal of Jilin Institute of Chemical Technology
关键词 杂化材料 MCM-41 化学改性 hybrid materials MCM-41 chemical modification
分类号 O621.25 [理学—有机化学]
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参考文献6

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共引文献9

同被引文献9

  • 1安群力,王水利.室温下介孔分子筛MCM-41的合成与表征[J].化工新型材料,2004,32(11):39-42. 被引量：10
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吉林化工学院学报
2010年 第4期

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