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HS-SPME-GC/MS分析花生油挥发性成分技术的优化 被引量:23

Optimazation of Solid-Phase Microextraction Conditions Combined with GC-MS for Analysis of Volatiles in Peanut Oil
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摘要 采用顶空固相微萃取结合气相色谱-质谱技术,建立了花生油挥发性成分分析方法。通过单因素分析得出最佳萃取条件为:PDMS-DVB萃取头,搅拌状态,萃取温度50℃,萃取时间40min,解吸时间5min。GC/MS初步分析鉴定出花生油挥发性成分53种。 The aim of this study was to establish an analysis method of aroma volatiles in peanut oil using headspace solid-phase microextraction combined with GC-MS.The optimum SPME conditions were determined and listed as follows: a PDMS-DVB fiber,magnetic stirring,the extraction temperature of 50 ℃,the extraction time of 40 min and the desorption time of 5 min.53 volatile compounds were then identified using the optimized HS-SPME condition combined with GC-MS.
出处 《食品与生物技术学报》 CAS CSCD 北大核心 2010年第4期500-507,共8页 Journal of Food Science and Biotechnology
基金 食用油质量安全控制技术研究与产业化示范项目(2009BADB9B08)
关键词 花生油 挥发性成分 固相微萃取 peanut oil volatile compounds solid-phase microextraction
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参考文献17

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