摘要
以四水合醋酸铜为原料,采用乙二醇回流法首先制备出氧化亚铜微球,然后以氧化亚铜为模板,在室温下制备出具有中空结构的硫化亚铜微球。利用现代分析手段对产物的尺寸、形貌、晶体结构以及成分进行了表征,并探讨了中空结构Cu2S微球的形成机理。
In this paper, Cu （ CH3 COO ） 2 · 4H2O is employed to prepare Cu2O microspheres in boiling ethylene glycol solution. Based on Cu2O, Cu2S microspheres with hollow structure are successfully synthesized at room temperature. The structural features and morphology of the product are characterized by means of modern analytical methods. A possible formation mechanism of the hollow microspheres is also briefly discussed.
出处
《现代化工》
CAS
CSCD
北大核心
2010年第9期56-58,60,共4页
Modern Chemical Industry
关键词
Cu2S微球
中空结构
CU2O
制备
机理
Cu2 S microspheres
hollow structure
Cu2 0
preparation
mechanism
