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硅基铌掺杂Bi_4Ti_3O_(12)薄膜溶胶-凝胶工艺的制备及铁电性改善研究

Research on Nb-doped Bi_4Ti_3O_(12) Prepared on p-Si with Sol-Gel
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摘要 采用溶胶-凝胶(Sol-Gel)法制备了铌元素(Nb)取代Ti元素的Bi4Ti3O12(BTN)铁电薄膜,研究不同掺杂浓度,不同退火温度等工艺对BTN薄膜的微观特性及剩余极化强度、矫顽场等电性能的影响。研究表明,650℃进行退火的BTN薄膜生长形态,晶粒开始呈棒状生长;当温度高于850℃时,薄膜的c轴生长取向增长趋势不再明显。铁电性方面,对Ti进行2%掺杂取代的BTN薄膜的铁电性能最佳。从而获得了BTN薄膜制备的合理工艺参数。 In order to master the correct techniques, in this experiment, we use sol-gel meth- od to prepare BIT film to research the anneal temperature's effects on the micro-structure of the film. The research shows that with the growth of the temperature, c-orientation of BIT is improved. The particles in the BIT film begins to grow in the form of stick-like structure with the annealing temperature is higher than 650℃. When the annealing temperature is higher than 850℃, the trend of e orientation growth become not so obvious.
出处 《信息记录材料》 2010年第5期28-32,共5页 Information Recording Materials
关键词 铁电薄膜 钛酸铋Bi4Ti3O12(BIT) 退火温度 ferroelectric Bi4Ti3O2 anneal temperature
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