邻氯苯甲酰肼缩水杨醛Schiff碱及其配合物的合成与表征

Synthesis and Characterization of Salicylaldehyde o-Clorobenzoylhydrazone Schiff Base and Its Metal Complexes

合成了邻氯苯甲酰肼缩水杨醛及Zn()、Co()、Ni()配合物,通过元素分析、红外光谱、紫外光谱、核磁共振氢谱对化合物进行了表征,用X射线单晶衍射测定邻氯苯甲酰肼缩水杨醛的晶体结构。

Salicylaldehyde o-clorobenzoylhydrazone（H2L）and its complexes with zinc（Ⅱ）,cobalt（Ⅱ）and nickel（Ⅱ）have been synthesized and characterized by elemental analyses,IR,UV-Vis and 1H NMR spectra.The crystal structure of salicylaldehyde o-clorobenzoylhydrazone has been determined by X-ray single crystal diffraction.