活血降酶散质量标准研究

Studies on Quality Standards for Huoxuejiangmei Powder

目的:建立活血降酶散的质量标准。方法:采用薄层色谱法鉴别组方中五味子、红花、丹参3味药;采用高效液相色谱法测定组方中主药丹参所含药理活性成分丹参酮ⅡA的含量。结果:薄层色谱鉴别斑点清晰;丹参酮ⅡA进样量在0.026 67～0.213 4μg线性良好,平均回收率为101.19%,RSD 1.18%。结论:所用方法简单、准确,可有效控制和血降酶散的质量。

Objective：To establish the quality standards for Huoxuejiangmei powder.Method： TLC method was used for identification of Fructus Schisandra Chinensis,Flos Carthami and Radix et Rhizoma Salviae Miltiorrhizae;and HPLC methods was used for the contents of tanshinone ⅡA in Radix et Rhizoma Salviae Miltiorrhizae in Huoxuejiangmei powder.Result： TLC method was simple,specific reproducible;HPLC method established was simply and accurate.TanshinoneⅡA was linear in the rang of 0.026 67-0.213 4 μg.The average recovery was 101.19%（RSD 1.18%）.Conclusion： This quality standard can control the quality of Huoxuejiangmei Powder effectively.