摘要
利用硅胶、sephadex LH-20、反相柱层析和制备液相等方法对独角莲水溶性成分进行研究,分离得到4个化合物,其结构经波谱方法和标准品对照鉴定为5-羟甲基糠醛(5-hydroxymethyl-2-furaldehyde)(1),腺苷(adenosine)(2),甘露醇(mannitol)(3)和核糖醇(ribitol)(4)。这些化合物均首次在独角莲化学成分研究中报道。
Four constituents were isolated from the Typhonium giganteum.The pure products were isolated by column chromatography of silica gel,Sephadex LH-20,ODS,and preparing HPLC.And their chemical structures were elucidated as 5-hydroxymethyl-2-furaldehyde(1),Adenosine(2),mannitol(3) and ribitol(4)by NMR spectroscopic evidence and compared with the standards sample.All Compounds are obtained from this plant for the first time.
出处
《中国野生植物资源》
2010年第6期38-39,共2页
Chinese Wild Plant Resources
关键词
独角莲
水溶性成分
分离
Typhonium giganteum
water soluble constituents
isolation