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Yb^(3+):Na_5Bi(WO_4)_2(MoO_4)_2多晶料的制备与性能表征 被引量：2

Synthesis and Characterization of Polycrystalline Material Yb^(3+):Na_5Bi(WO_4)_2(MoO_4)_2
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摘要 采用高温固相反应合成了混酸盐多晶材料Yb3+:Na5Bi(WO4)2(MoO4)2。利用X射线衍射仪(XRD)、同步热分析仪(DSC-TG)、红外光谱仪和荧光光谱仪等分析测试技术,对多晶材料Yb3+:Na5Bi(WO4)2(MoO4)2的结构与光谱性能进行了研究,研究发现:新相属于四方晶系,空间群为I41/a(88),熔点约为930℃,吸收带宽为83 nm,发射中心波长为1006 nm,发射带宽为50 nm,荧光寿命为589.03μs。 In order to research in the novel laser crystal of molybdate,the compound-anion polycrystalline material Yb3＋：Na5Bi（WO4）2（MoO4）2 was synthesized by solid state reaction.The material was characterized by XRD,DSC-TG,absorption spectrum and emission spectrum.The result is concluded that the new phosphor belongs to tetragonal,and space group is I41/a（88）.Its melt point is about 930 ℃ and the absorption band,emission band,center emission wavelength is about 83 nm,50 nm,1006 nm respectively.
作者 付乔克 韩永飞 陈振强 李安明 朱思祁
机构地区 暨南大学光电工程研究所 暨南大学光电信息与传感技术广东普通高校重点实验室
出处 《硅酸盐通报》 CAS CSCD 北大核心 2010年第6期1275-1279,共5页 Bulletin of the Chinese Ceramic Society
基金 广东省自然科学基金(9178922035-X000002) 中科院光电材料化学与物理重点实验室开放基金(2009KL006)
关键词 激光晶体 多晶材料 制备与表征 钼酸盐 Yb3+:Na5Bi(WO4)2(MoO4)2 laser crystal polycrystalline material synthesis and characterization molybdate Yb3＋：Na5Bi（WO4）2（MoO4）2
分类号 O734 [理学—晶体学]
  • 相关文献

参考文献13

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  • 2Voron'ko Yu K,Subbotin K A,Shukshinet V E,et al.Growth and spectroscopic investigations of Yb3+-doped NaGd(MoO4)2 and NaLa(MoO4)2-new promising laser crystals[J].Optical Materials,2006,29:246-252.
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二级参考文献13

  • 1Kuzmicheva G M, Lis D A, et al. Growth and structural X-ray investigations of scheelite-like single crystals Er, Ce : NaLa( MoO4 ) 2 and Yb : NaGd ( WO4 ) 2 [ J ]. Journal of Crystal Growth, 2005,275 : 1835-1842.
  • 2Voronko Yu K, Subbotin K A, et al. Growth and spectroscopic investigations of Yb^3+ -doped NaGd( MoO4 ) 2 and NaLa( MoO4 ) 2-new promising laser crystals [ J]. Optical Materials,2006,29:246-252.
  • 3Cascales C, Mendez Blas A, Rico M, et al. The optical spectroscopy of lanthanides R^3+ in ABi( XO4 ) 2 ( A = Li, Na; X = Mo, W) and LiYb (MoO4) 2 multifunctional single crystals:Relationship with the structural local disorder [ J]. Optical Materials ,2005,27:1672-1680.
  • 4Fernandez J, Illarramendi M A, Iparraguirre I, et al. Rb5 Nd ( MoO4 ) 4 a self-tunable birefringent laser crystal [ J ]. Optical Materials, 2004,26:483- 487.
  • 5Li X Z, Lin Z B, Zhang L Z, et al. Growth and spectral properties of Yb^3+ -doped NaY ( MoO4 ) 2 crystal [ J ]. Optical Materials,2007,29:728 -731.
  • 6Li X Z, Lin Z B, Zhang L Z, et al. Growth, thermal and spectral properties of Nd^3+ -doped NaGd ( MoO4 ) 2 crystal [ J ]. Journal of Crystal Growth, 2006,290:670-673.
  • 7Huang X Y, Hu Z S, Lin Z B, et al. Growth and up-conversion emission of Er^3+/Yb^3+ -codoped LiGd ( MoO4 ) 2 crystal [ J ]. Journal of Crystal Growth ,2005,276 : 177-181.
  • 8Femandez-Martynez F, Colon C, Montero J L, et al. Synthesis and characterization of LnAg( WO4 ) ( MoO4 ) [ J]. Journal of alloys and compounds, 2008, 451:317-319.
  • 9Zatovsky I V, Terebilenko K V, Slobodyanik N S, et al. Synthesis, characterization and crystal structure of K2 Bi ( PO4 ) ( MoO4 ) [ J ]. Journal of Solid State Chemistry,2006,179:3550-3555.
  • 10Xu L M, Chen J Z. Growth, structure and spectral characteristics of NaY ( W0. 5 Mo0. 2 O4 ) 2 crystal [ J ]. Journal of Crystal Growth, 2007,306 : 311 - 315.

共引文献14

同被引文献12

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  • 3Tomaszewicza E,Dabrowska G,Kaczmarek SM,et al.Solid-state Synthesis And Characterization of New Cadmium and Rare-earth MetaI Molybdato-Tungstates Cd0.25 RE0.50(MoO4)0.25(WO4)0.75(RE = Pr,Nd,Sm-Dy)[J].Journal of Non-Crystalline Solids,2010,(356):2059.
  • 4Chiu C H,Wang M F,Lee CS,et al.Structural,Spectroscopic and Photoluminescence Studies of LiEu(WO4)2-x(MoO4)x As A Near-UV Convertible Phosphor[J].Journal of Solid State Chemistry ,2001,180:619.
  • 5Cao F B,Tian Y W,Li L S,et al.Preparation of Eu^3 + /Y^3 + Co-doping Red-emitting Phosphorsfor White-light Emitting Diodes(W-LEDs)Application and Investigation of Their Optical Characteristics[J]. Mater Electron ,201l,22:510.
  • 6Yan Y,Cao F B,Tian Y W,Li L S.Improved Luminescent Properties of Red-emitting Eu^3 + /Y^3 +:Ca0.54 Sr0.34-1.5x Eu0.08 Yx(MoO4)y(WO4)1-y Phosphor for LED Application by Charge Compensation[J].Journal of Luminescence,2011,131:1140.
  • 7Zeng L,Tang W J.Synthesis and Luminescence Properties of Red-emittfng Phosphors NaY 0.87Eu0.13(WO4)1.2(MoO4)0.8 [J] .Physica By 2011,(406):2901.
  • 8刘波,张行愚,王青圃,李述涛,苏富芳,贾鹏.LD抽运Nd∶YVO_4自喇曼倍频黄光激光器[J].光子学报,2007,36(10):1777-1780. 被引量：8
  • 9张艳,宫慧丽,石士考,周济,叶建平.亚微米级红色荧光粉NaEu(MoO4)2的水热合成及光谱特性[J].无机化学学报,2009,25(3):563-566. 被引量：11
  • 10胡志朋,付乔克,陈振强.Sm^(3+)∶Na_5Y(MoO_4)_4材料的多晶合成与性能表征[J].人工晶体学报,2011,40(6):1414-1417. 被引量：8

引证文献2

二级引证文献3

硅酸盐通报
2010年 第6期

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