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2,4-二氯-5-炔丙氧基苯胺的合成 被引量:2

Synthesis of 2, 4 dichloro 5 propargyloxyaniline
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摘要 以2 ,4二氯5硝基苯酚为原料经醚化、还原得到2 ,4二氯5炔丙氧基苯胺, 总收率达80 % ( 以2 ,4二氯5硝基苯酚计) 。并对产品及其合成中间体进行了红外光谱分析。 dichloro 5 propargyloxyaniline, an important intermediate of the herbicides Oxadiargyl, was synthesized by the etherization and reduction of 2, 4 dichloro 5 nitrophenol with total recovery of 80%. The product and intermediate were analyzed by infrared spectrum.
出处 《湖南化工》 1999年第5期26-26,30,共2页
关键词 二氯 炔丙氧基苯胺 合成 红外光谱 除草剂 dichloro 5 propargyloxyaniline synthesis infrared spectrum
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参考文献1

  • 1章思归.精细有机化工制备手册[M].北京:科学技术文献出版社,1994.130-131.

同被引文献19

  • 1林长福,马宏娟,李鸣,高爽,杨玉廷.丙炔噁草酮对水稻的药害试验研究[J].现代农药,2004,3(3):17-19. 被引量:7
  • 2冯化成译.农药译丛,1989,11(6):55-55.
  • 3GITSOPOULOS T K, WILLIAMS F R J. Effects of Oxadiargyl on Direct-seeded Rice and Echinochloa crus-galli under Aerobic and Anaerobic Conditions[J]. European Weed Research Society Weed Research, 2004(44): 329-334.
  • 4MALTY S K, PRAHAM N C, PATWARDHAN A V. Kinetics of the Reduction of Nitroluenes by Aqueous Ammonium Sulfide under Liquid-liquid Phase Transfer Catalysis[J]. Applie Catalysis A: General, 2006, 301: 251-258.
  • 5YADAV G D, JADHAV Y B, SENGUPTA S. Selectivity Engineered Phase Transfer Catalysis in the Synthesis of Fine Chemicals: Reactions ofp-Chloronitrobenzene with Sudium Sulphide[J]. Journal of Molecular Catalysis A: Chemical, 2003, 200(1): 117-129.
  • 6JOSHI M V, MUKESH D. Transfe Hydrogenation of Niro Compounds with Heteropolyaeid Catalysts[J]. Journal of Catalysis, 1997, 168(2): 273-277.
  • 7AGRAWAL A, TRATNYEK P G, Reduction of Nitro AramaticCompounds by Zero-valent Iron Metal[J]. Environ Sci Technol, 1996, 30(1): 153-160.
  • 8PRAROOD S. Mg-Fe Hydrotalcite as a Catalyst for the Reduction of Aromatic Nitro Compounds with Hydrazine Hydrate[J]. Journal of Catalysis, 2000, 191(2): 467-473.
  • 9JOHN W, MICHAEL L, SIDOVAR M, et al. Mechanism of the Carbon Catalyzed Reduction of Nitrobenzene by Hydrazine[J]. Carbon, 2000, 38: 655-661.
  • 10DHAKSHINAMOORTHY A, PITCHUMANI K. Clay Entrapped Nickel Nanoparticlcs as Efficient and Rccyclable Catalysts for Hydrogenation of Olefins[J]. Tetrahcdron Letters, 2008, 49: 1818- 1823.

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