摘要
目的:建立活血舒筋贴膏剂的质量标准。方法:采用薄层色谱(TLC)法对没药挥发油进行鉴别;采用高效液相色谱法对制剂中紫丁香苷进行含量测定。结果:TLC斑点清晰,分离度好;紫丁香苷进样量在0.138～0.690μg范围内与峰面积积分值呈良好线性关系(r=0.9999),平均回收率为98.50%,RSD=3.04%(n=6)。结论:所建标准可用于活血舒筋贴膏剂的质量控制。
OBJECTIVE： To establish the quality standard for Huoxue shujin plaster. METHODS： The volatile oil of Commiphora Myrrha was identified by TLC and the content syringin was determined by HPLC. RESULTS： The TLC spots were clear and well-separated. The linear range of syringin in Huoxue shujita plaster was 0,138-0.690 mg （r=0.999 9） with an average recovery of 98.50 % （RSD = 3.04 %, n = 6）. CONCLUSION： The method was reproducible for the quality control of Huoxue shujin plaster.
出处
《中国药房》
CAS
CSCD
北大核心
2011年第11期1012-1014,共3页
China Pharmacy
基金
深圳市科技计划立项项目(201003186)
