摘要
目的:研究中药制剂妇炎宁胶囊的质量标准。方法:采用TLC对丹皮、延胡索、桂枝、赤芍等成分进行色谱鉴别,HPLC测定丹参酮ⅡA 的含量。结果:TLC鉴别方法专属性强。含量测定丹参酮ⅡA 在0.102μg~0 .510μg 间有良好的线性关系。回收率为96 .47 % ,RSD% 为2 .37 % 。结论:本质量标准可有效地控制妇炎宁胶囊的质量。
OBJECTIVE:To study the quality standard of Fuyanning capsule.METHODS:Thin layer chromatography was used for simultaneously identification of Cortex Moutan,Rhizoma Corydalls,Ramulus Cinnamomi and Radix Paeoniae Rubra.HPLC was used for the determination of tanshinone Ⅱ A.RESULTS:The TLC identification was highly specific and the spots were clear and concentrated.The linearity for tanshinone Ⅱ A was obtained over the range of 0.102~0.510μg.The average recovery of Tanshinone Ⅱ A was 96.47% with RSD 2.37%.CONCLUSION:This quality standard was capable of effectively controling the quality of Fuyanning capaule.
出处
《中国药学杂志》
CAS
CSCD
北大核心
1999年第11期766-769,共4页
Chinese Pharmaceutical Journal
关键词
妇炎宁胶囊
丹皮
延胡索
桂枝
中药
质量标准
Fuyanning capsule,Cortex Moutan,Rhizoma Corydalia,Ramulus Cinnamomi,Radix Paeoniae Rubra,tanshinone Ⅱ A,HPLC