摘要
目的:建立GC法测定鼻通宁滴剂中挥发油的含量。方法:采用聚乙二醇(PEG)-20M为固定相,涂布浓度为10%,70-110℃,初温保持1分钟,每分钟升高5℃,终温保持8分钟。结果:方法线性关系良好(r=0.9999);检测限3.43ng。结论:本法简便、准确、专属性强,可用于鼻通宁滴剂中挥发油的含量测定。
Objective:To establish GC method for determination of Volatile oil content in Bitongning drops.Methods:using polyethylene glycols(PEG)-20M for stationary phase,coating,70 ~ 10% for concentration,temperature keeping early 110℃ 1 minute,every minute,elevated temperature keep ℃ 8 minutes.Results:linear(r = 0.9999),Detection limit higher 3.43 ng.Conclusion:This method is simple and accurate,and can be used for determination of Volatile oil Content in Bitongning drops.
出处
《黑龙江医药》
CAS
2011年第1期16-17,共2页
Heilongjiang Medicine journal
关键词
鼻通宁滴剂
挥发油
气相色谱
含量测定
Bitongning drops
Volatile oil
gas chromatography
content determination