4,4,4-三苯基-1-丁烯-3-酮的合成研究

Synthesis of 4,4,4-triphenyl-1-butlene-3-one

从三苯甲烷出发经过甲酰化,再与乙烯基溴化镁加成,氧化,高收率的合成了标题化合物。同时,对各步反应的实验条件进行了优化,找到了较好的合成条件,并用1HNMR和13CNMR对各步产物进行了表征。

4,4,4-Triphenyl-1-butlene-3-one was synthesized from triphenylmethane via formulation,addition reaction and oxidation.The suitable reaction conditions were obtained and structures of the products were identified by 1HNMR and 13CNMR.