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醋酸溶液中2,3-二芳基-喹喔啉的简便合成 被引量:2

A Simple and Efficient Synthesis of 2,3-Diarylquinoxaline in Acetic Acid
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摘要 1,2-二芳基乙二酮与1,2-苯二胺在室温醋酸溶液中反应数分钟,生成2,3-二芳基-喹喔啉.反应时间短(1~10 min),产率高(90%~97%),反应条件温和,操作简便. Synthesis of 2,3-diarylquinoxaline via the condensation of 1,2-diarylethanedione and 1,2-phenylenediamine was carried out in excellent yields(90%~97%) in acetic acid at room temperature within 1~10 min.This method provides several advantages such as short reaction time,high yields,simple operation and mild conditions.
出处 《有机化学》 SCIE CAS CSCD 北大核心 2011年第3期365-367,共3页 Chinese Journal of Organic Chemistry
基金 河北省自然科学基金(No.B2006000969)资助项目
关键词 喹喔啉 合成 1 2-二芳基乙二酮 缩合反应 催化 quinoxaline synthesis 1 2-diarylethanedione condensation catalysis
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  • 1Lindsley, C. W,; Zhao, Z.; Leister, W. H.; Robinson, R. G.; Barnett, S. F.; Defeo-Jones, D.; Jones, R. E.; Hartman, G. D.; Huff, J. R.; Huber, H. E.; Duggan, M. E. Bioorg. Med. Chem. Lett. 2005, 15, 761.
  • 2Seitz, L. E.; Suling, W. J., Reynolds, R. C. J. Med. Chem. 2002, 45, 5604.
  • 3Brock, E. D.; Lewis, D. M.; Yousaf, T. L; Harper, H. H. WO 9951688, 1999 [Chem. Abstr. 1999, 131, 287743b].
  • 4Dailey, S.; Feast, J, W.; Peace, R. J.; Till, I. C.; Sage, S.;Wood, E. L. J. Mater. Chem. 2001, 11, 2238.
  • 5O'Brien, D.; Weaver, M. S.; Lidzey, D. G.; Bradley, D.D. C. Appl. Phys. Lett. 1996, 69, 881.
  • 6Crossley, J. C.; Johnston, L. A. Chem. Commun. 2002, 1122.
  • 7Cai, J.-J.; Zou, J.-P.; Pan, X.-Q.; Zhang, W. Tetrahedron Lett. 2008, 49, 7386.
  • 8Heravi, M. M.; Taheri, S.; Bakhtiari, K.; Oskooie, H. A. Catal. Commun. 2007, 8, 211.
  • 9More, S. V.; Sastry, M. N. V.; Wang, C.-C., Yao, C.-F. Tetrahedron Lett. 2005, 46, 6345.
  • 10Heravi, M. M.; Tehrani, M. H.; Bakhtiari, K.; Oskooie, H. A. Catal. Commun. 2007, 8, 1341.

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  • 1Seitz L,Suling W, Reynolds R. Synthesis of new qui-noxa- line-2-carboxylate 1,4-dioxide derivatives as anti-applica- tion of sulfamic acid in organic synthesis mycobacterium tuberculosis agents [ J ]. J Med Chem , 2002,45 : 5 604-5 606.
  • 2He W, Myers M, Hanney B. Potent quinoxaline-bascd in- hibitors of PDGF receptor tyrosine kinase activity. Part 2 : the synthesis and biological activities of RPR127963 an o- rally bioavailable inhibitor [ J ]. Bioorg Med Chem Lett, 2003,13:3 097-4 000.
  • 3Lindsley C, Zhao Z ,Leister W. Allosteric Akt(PKB) inhib- itors: discovery and SAR of isozyme selective inhibitors [ J ]. Bioorg Med Chem Lett ,2005,15:761-764.
  • 4Mizuno T, Wei W, Eller T, et al. Phenanthroline Comple- xes bearing fused dipyrrolylquinoxaline anion recognition sites:efficient fluoride anion receptors [ J ]. J Am Chern Soc,2002,124:1 134-1 135.
  • 5Dailey S, Feast J W, Peace R J, et al. Synthesis and device characterisation of side-chain polymer elegtron transport materials for organic semiconductor applications [ J ]. J Mater Chem ,2001,11:2 238-2 243.
  • 6Jonathan L S, Hiromitsu M,Toshihisa M, et al. Quinoxa- line-oligopyrroles: improved pyrrole-based anion receptors [J]. Chem Commun,2002, (8) :862-863.
  • 7Peter P, Gang Z, Grace A, et al. Quinoxaline excision : a novel approach to tri-and diquinoxaline cavitands [ J ]. Org Lett ,2004,6:333-336.
  • 8Taylor E, Wipf P. The chemistry of heterocyelic compounds [ M ]. New York: JohnWiley&Sons ,2004, vol. 61 : 16-44.
  • 9More S, Sastry M, Yao C. Cerium (IV) ammonium nitrate (CAN) as a catalyst in tap water:A simple,proficient and green approach for the synthesis of quinoxalines [ J ]. Green Chem ,2006,8:91-95.
  • 10Srinivas C, Kumar C, Rao, V, et al. Efficient, convenient and reusable po:yaniline-suifate salt cata:tys't for the syn- thesis of quinoxaline derivatives [ J ]. J Mol Catal A: Chem ,2007,265:227-230.

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