摘要
溴化铜的溴代反应结果表明:在反应温度为60℃,原料的摩尔配比为4-氨基-3,5-二氯苯乙酮∶溴化铜=1∶2,反应2.2h合成标题化合物。
The results of cupric bromide as brominating agent in the bromo-reaction indicated that the target compound was synthesized by the mole rate of 4-amino-3,5-dichloroacetophenone and cupric bromide was 12 at 60 for 2.2 hours with a yield rate over 95%.
出处
《化学研究》
CAS
1999年第2期35-37,共3页
Chemical Research