摘要
采用甲醇振荡提取-高效液相色谱法测定(HPLC),对白蚁防治药剂吡虫啉在武汉建筑用地3种特征土壤中的残留量进行阳性添加和回收率测定试验。结果表明:吡虫啉在各种土壤中回收率和变异系数分别为潮土73.7%~78.8%,2.2%~3.4%,红棕壤67.8%~72.2%,2.8%~4.5%,黄棕壤66.4%~70.1%,2.5%~3.8%。
The Determination of Recovery Rates of Imidacloprid in three Characteristics of Wuhan Architecture Soils by Methanol oscillation extraction-- HPLC method. The determination results indicated that the recovery rates and CV of Imidacloprid are 73.7%-78.8% and 2.2% - 3.4% for chao soil,67.8%-72.2% and2.8%-4.5%for red brown soil, 66.4 % - 70.1% and 2.5 % - 3.8 % for yellow brown soil, respectively.
关键词
吡虫啉
武汉建筑用地特征土壤
甲醇振荡提取-高效液相色谱法
回收率测定
Imidacloprid
Characteristics of Architecture Wuhan Soils
Methanol oscillation extraction--HPLC
determination of recovery rates