摘要
报道了用硅酮固定液ＯＶ－１７改性，以自制的非水溶性β－环糊精聚合物为固定相，采用超动态法制备出柱效高，热稳定性好的弹性石英毛细管柱。对毛细管柱的活性、极性、热稳定性等色谱性能进行了考察，已对一系列手性化合物进行拆分。
A flexible silica capillary column with excellent column efficiency and thermal stability was prepared with β cyclodextrin polymer modified by methyl phenyl(50∶50) silicone as stativnary phase by superdynamical coating method.By using this column a series of enantiomers have been separated and its performance has been investigated.Satisfactory resulst have been oltained.
出处
《分析试验室》
CAS
CSCD
1999年第6期85-86,共2页
Chinese Journal of Analysis Laboratory
关键词
毛细管柱
手性毛细管柱
β-环瑚精
聚硅氧烷
cyclodextim polymer
modified by methyl phenyl (50∶50) siliane
chiral capillary column
