摘要
目的:测定不同地区市售乳香中乙酸辛酯的含量。方法:采用气相色谱法HP-6890气相色谱仪;FID检测器;毛细管色谱柱HP INNOWAX(30m×0.53mm×1.0μm);色谱条件:进样口温度:230℃;柱程序升温:130℃(3min)-30℃/min-200℃(4min);检测器温度:250℃;载气流速(N2):6.3mL/min;进样量:1.0μL。结果:线性范围0.5~2.0μg,r=0.9990。结论:5个不同地区乳香挥发油中乙酸辛酯的含量无明显差异。
Objective:To determine Octyl Acetate in Olibanum of different regions.Methods:To use HP-6890 with detector FID and capillary column HP INNOWAY(30m×0.53mm×1.0μm).Chromatographic conditions:Temperature of the meatus for injecting samples is 230℃,programmed temperature gas chromatography:130℃(3min)-30℃/min-200℃(4min).The detector temperature was 250℃.The gas flow-rate(N2)was 6.3mL/min.The injection volume was 1.0 μL.Result:The linear range was 0.5~2.0μg,r=0.9990.Conclusion:The contents of Octyl Acetate in Olibanum from 5 different regions have no significant differences.
出处
《中医药学报》
CAS
2011年第2期76-77,共2页
Acta Chinese Medicine and Pharmacology
基金
国家"十一五"科技支撑项目-中药饮片炮制技术和相关设备研究-乳香饮片醋炙和相关设备研究(编号:2006BAI09B06-07-3)
关键词
乳香
乙酸辛酯
GC法
Olibanum
Octyl Acetate
GC method