毛杜仲藤皮的化学成分(英文)

Chemical Constituents of Parabarium huaitingii

目的:研究毛杜仲藤皮的化学成分。方法:用硅胶,制备薄层层析等手段进行分离纯化,根据化合物的理化性质和光谱数据鉴定结构。结果:分离并鉴定了9个化合物,即大黄素甲醚(1),延胡索酸(2),龙胆酸甲酯(3),丁香酸甲酯(4),丁香酸(5),2,5-二甲氧基对苯醌(6),香草酸(7),3,4,5-三甲氧基苯甲酸(8),6-甲氧基-7-羟基香豆素(9)。结论:所有化合物均首次从该植物中分离得到。

AIM： To investigate the chemical constituents of Parabarium huaitingii. METHODS： The constituents were isolated and purified by silica gel column chromatography and preparative TLC. Their structures were identified on the basis of spectral data and physiochemical properties. RESULTS： Nine compounds were isolated and their structures were elucidated as physcion （1）, fumaric acid （2）, methyl gentisate （3）, 4-hydroxy-3, 5-dimethoxybenzoic acid methyl ester （4）, syringic acid （5）, 2, 5-dimethoxy-pbenzoquinone （6）, vanillic acid （7）, 3, 4, 5-trimethoxybenzoic acid （8） and 6-methoxy-7-hydroxycoumarin （9）. CONCLUSION： All of the compounds were isolated from this genus for the first time.