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N,N-TDD衍生物的合成

Synthesis of N,N-substitutes derivatives of TDD
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摘要 经过7步反应合成了两种N-(烷基)-TDD双取代衍生物配体NNEPTDD和NNEMPTDD,并对其进行了红外、核磁共振、质谱以及熔点等分析表征,结果表明合成的目标产物符合预期要求。 Two N-(alkyl)-derivatives of TDD(2,2,9,9-tetramethyl-4,7-diaza-1,10-decanedithiol) that NNEPTDD and NNEMPTDD were synthesized via seven steps reaction and their structures were confirmed by IR,HNMR,MS methods.The results showed that the synthesis was successful,and final products were ready to us for further investigations.
出处 《化学试剂》 CAS CSCD 北大核心 2011年第5期417-419,共3页 Chemical Reagents
基金 “核废物与环境安全”国防重点学科实验室开放基金资助项目(09zxsk02)
关键词 合成 NNEPTDD NNEMPTDD synthesis NNEPTDD NNEMPTDD
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  • 1孟昭兴,刘伯里.锝化学研究 Ⅵ.^(99)Tc^m-HM-PAO异构体稳定性的研究[J].核化学与放射化学,1993,15(1):6-11. 被引量:3
  • 2王文进,罗顺忠,何佳恒,王关全,杨玉青,魏洪源,蒋树斌,邴文增,蒲满飞,刘国平.^(188)Re-NEPTDD的制备及生物分布研究[J].核技术,2005,28(4):305-308. 被引量:1
  • 3魏毅,核化学与放射化学,1989年,11卷,2期,78页
  • 4DEMAIMAY F, DAZORD L, ROUCOUX A, et al. Rhenium-188 and Technetium-99m Nitridobis (N-ethoxy-N-ethyldithiocarbamate) Leucocyte Labeling Radiopharmaceuticals: [^188ReN ( NOET)2] and [^188TcN (NOET)2], NOET= Et(EtO) NCS2: Their in Vitro Localization and Chemical Behaviour[J]. Nucl Med Biol, 1997, 24(4): 701-705.
  • 5BOLZATI C, BOSCHI A, UCCELLI L, et al. Chemistry of the Strong Electrophilic Metal Fragment [^99Tc(N)(PXP)]^2+ ( PXP = Diphosphine Ligand): a Novel Tool for the Selective Labeling of Small Molecules [J]. J Am Chem Soc, 2002, 124:11 468-11 479.
  • 6ZHANG Junbo, WANG Xuebin, LIU Jing. Synthesis of a bis-(N-sec-butyl- dithiocarbamato)-nitrido-^99Tc^m Complex: a Potential New Radiopharmaceutical for Brain Perfusion Studies[J]. Appl Radiat Isot, 2005, 62: 33-37.
  • 7DEUTSCH E, LIBSON K, VANDERHEYDEN JL, et al. The Chemistry of Rhenium and Technetium as Related to Theuse of Isotopes of These Elements in Therapeutic and Diagnostic Nuclear Medicine[J]. Int J Rad Appl Instrum B, 1986, 13: 465-477.
  • 8JEONG JM, KIM YJ, LEE YS, et al. Lipiodol Solution of a Lipophilic Agent,188 Re-TDD, for the Treatment of Liver Cancer[J]. Nucl Med Biol, 2001, 28:197-204.
  • 9LEE YS, JEONG JM, KIM YJ, et al. Synthesis of ^188Re-labeled Long Chain Alkyldiaminedi-thiol for Therapy of Liver Cancer[J]. Nuel Med Commun, 2002, 23: 237-242.
  • 10LAMBERT B, BACHER K, KEUKELEIRE KD, et al. ^188Re-HDD/Lipiodol for Treatment of Hepatocellular Carcinoma: a Feasibility Study in Patients With Advanced Cirrhosis[J]. J Nuel Med, 2005, 46:1 326-1 332.

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