摘要
提出菜籽油油脚-皂脚水解-醇解、皂化复合裂解清洁工艺。得到的最佳工艺条件为:水解温度190℃,水解时间12h,水与油脚-皂脚体积比3∶1,黑脚醇解-皂解时间8h。脂基裂解率98%,脂肪酸得率96%,芥酸质量分数达95%
A cleaner process of hydrolysis alcoholysis,saponification compound splitting to rape oil foots soap foots was put forward. The optimum technological conditions were obtained: hydrolysis temperature,190℃;hydrolysis time,12h; volume ratio of water and oil foots soap foots,3∶1;alcoholysis saponification time of hydrolysis foots, 8h. Fat base splitting rate was 98%. The yield of fat acid was 96%. The purity of erucic acid reached 95%.
出处
《江苏化工》
1999年第4期19-21,共3页
Jiangsu Chemical Industry
基金
贵州省科学技术基金
关键词
菜油脚
皂脚
皂化
油脚
脂肪酸
Rape oil foots Rape soap foots Erucic acid Hydrolysis Alcoholysis Saponification