摘要
以邻二甲苯为原料，经五步反应合成了四甲基［双（３，４二甲酸酐苯基）］二硅氧烷（Ⅴ）．（Ⅴ）与八甲基环四硅氧烷平衡，得到含数个硅氧链段的芳香二酐．
Starting from 4 bromo o xylene,1,3 bis(3,4 dicarboxyphenyl) 1,1,3,3 tetramethyldisiloxane dianhydride(Ⅴ) was synthesized.(Ⅴ) was equilibrated with octamethylcyclotetrasiloxane used sulfuric acid as a catalyst,aromatic dianhydride containing siloxane was obtained.
出处
《山东大学学报（自然科学版）》
CSCD
1999年第1期74-77,共4页
Journal of Shandong University(Natural Science Edition)
关键词
含硅芳香二酐
硅氧烷
有机硅化合物
合成
silicon containing aromatic dianhydride
1,3 bis(3,4 dicarboxyphenyl) 1,1,3,3 tetramethyldisiloxane dianhydride
organic silicon
