摘要
以三光气和甲氧基乙酸为原料,用三光气法合成了纯度较高的甲氧基乙酰氯。探讨了催化剂及用量、反应溶剂、投料比等因素对三光气法合成了甲氧基乙酰氯反应收率的影响。
The high purity methoxyacetyl chloride was synthesized using methoxyacetyl acid and triphosgene as raw materials.The effect factors include catalyst regent and its quantity,solvent,reactant ratio are discussed.
出处
《科学技术与工程》
2011年第16期3848-3849,3857,共3页
Science Technology and Engineering
关键词
三光气
甲氧基乙酰氯
甲氧基乙酸
triphosgene methoxyacetyl chloride methoxyacetyl acid
