摘要
由水合肼、CS2与取代的溴化苄在低温条件下反应,合成肼基二硫代甲酸苄酯类化合物,再在无水乙醇体系中及高温回流条件下与取代的水杨醛进行反应,合成了一系列标题化合物,其结构经质谱、紫外光谱、红外光谱、元素分析及1H核磁共振等进行表征。
Hydrazine dithiocarbamate benzyl ester was synthesized by reaction of the hydrazine hydrate,CS2 and substituted benzyl bromide at low temperature.Then a series of substituted salicylidene condensation hydrazine dithiocarbamate benzyl esters were synthesized at high temperature reflowing with absolute ethanol as solvent.The structures of samples were confirmed by MS,UV,IR and elemental analysis.
出处
《化学试剂》
CAS
CSCD
北大核心
2011年第6期500-502,共3页
Chemical Reagents
基金
2008年浙江省大学生科技创新项目(浙教高教[2009]30号)
