摘要
采用液相合成法,实现了多晶硒化锌微米空心球的低温合成。通过扫描电镜选观察到直径在1~4μm左右的ZnSe多晶微米空心球体。用XRD(X射线衍射)测定样品的成分,对样品纯度进行鉴定。用紫外可见光谱对实验样品分析,发现有明显蓝移现象。
The liquid-synthesis method was used to prepare the micro-hollow-bead of polycrystal ZnSe under relatively low temperature.By the method of scan electron microscope(SEM),the micro-hollow-bead with 1~4 ?m diameters was observed.By XRD(X-ray Diffraction),ingredient of the sample was determined,and purity of the sample was identified.Then the sample was analyzed by UV-vis spectrum,the blueshife phenomenon was clearly found.
出处
《辽宁化工》
CAS
2011年第6期569-571,共3页
Liaoning Chemical Industry
基金
安徽省2010高校优秀青年人才基金项目
项目号:2010SQRL163
关键词
硒化锌
微米晶
液相合成
Zinc selenide
Microcrystalline
Lquid-synthesis method