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ZnSe微米晶的液相合成及表征

Liquid-phase Synthesis and Characterization of ZnSe Microcrystal
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摘要 采用液相合成法,实现了多晶硒化锌微米空心球的低温合成。通过扫描电镜选观察到直径在1～4μm左右的ZnSe多晶微米空心球体。用XRD(X射线衍射)测定样品的成分,对样品纯度进行鉴定。用紫外可见光谱对实验样品分析,发现有明显蓝移现象。 The liquid-synthesis method was used to prepare the micro-hollow-bead of polycrystal ZnSe under relatively low temperature.By the method of scan electron microscope（SEM）,the micro-hollow-bead with 1～4 ？m diameters was observed.By XRD（X-ray Diffraction）,ingredient of the sample was determined,and purity of the sample was identified.Then the sample was analyzed by UV-vis spectrum,the blueshife phenomenon was clearly found.
作者 李莉 李天佑
机构地区 淮南师范学院化学与化工系
出处 《辽宁化工》 CAS 2011年第6期569-571,共3页 Liaoning Chemical Industry
基金 安徽省2010高校优秀青年人才基金项目 项目号:2010SQRL163
关键词 硒化锌 微米晶 液相合成 Zinc selenide Microcrystalline Lquid-synthesis method
分类号 TQ462.24 [化学工程—制药化工]
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参考文献8

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共引文献10

辽宁化工
2011年 第6期

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