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孜然精油的层析分离及GC-MS分析 被引量:2

Column Chromatography Separation and GC-MS Determination of Essential Oil Components of C.cyminum L.
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摘要 [目的]分离孜然(Cuminum cyminumL.)精油,并对其成分进行分析,为其应用奠定基础。[方法]采用低沸点有机溶剂的索式抽提得到孜然精油,并用柱层析法对精油进行了组分分离、GC-MS进行组分的定性和定量分析。[结果]以石油醚为溶剂的孜然精油的提取工艺为:加热温度33℃,抽提时间10 h;采用柱层析可以有效地将孜然精油分为饱和烃、芳烃、非烃和胶质4种组分。[结论]该研究确定了孜然精油中对食品防腐具有抑菌活性的主要成分。 [Objective] The research aimed to separate the essential oil of C.cyminum L.,and analyze its components,to lay a experimental foundation for its applications.[Method] Essential oil was extracted from C.cyminum L.by using low boiling-point organic solvents and was separated and identified by Column Chromatography and GC-MS.[Result] The results showed that optimum petroleum ether extraction conditions for essential oil were as follows: Extraction temperature 33 ℃,extract time 10 h.The essential oil could be separated from four chemical components: Aliphatics,aromatics,nonhydrocarbon and pectin.[Conclusion] The study confirms the main components from essential oil of C.cyminum L.restrained bacterium in foodstuff antisepsis.
出处 《安徽农业科学》 CAS 北大核心 2011年第16期9840-9841,9955,共3页 Journal of Anhui Agricultural Sciences
关键词 孜然 精油 抽提 层析 GC-MS C.cyminum L. Essential oil Extraction Column chromatography GC-MS
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