N-氰基-亚胺酯衍生物的合成新方法

A New Method for the Synthesis of N-cyanoimidate Derivatives

以甲醇为溶剂,N-溴代丁二酰亚胺为氧化剂,单氰氨和β-硝基芳基乙烯为原料,合成了一系列N-氰基-亚胺酯衍生物,其结构经1HNMR,13CNMR和HR-MS确证。

A series of N-cyanoimidate derivative were synthesized from cyanamide and β-nitryl-arylethylene by a new method of using NBS as the oxidant and methanol as the solvent.The structures were confirmed by 1H NMR,13CNMR and HR-MS.