摘要
介绍了一种简单实用的合成双二苯基膦烷烃的方法,并详细报道了合成路线,讨论了影响产率的各种因素。对最终产物进行了核磁表征,并对核磁谱图进行了解析。
One simple and practical method for the synthesis of di (diphenylphosphine) - alkanes was introduced, and the synthesis route was reported in detail. Some influence factors were discussed here. Final products detected by 1↑H NMR, and 31↑P NMR were analysed.
出处
《山东化工》
CAS
2011年第7期27-29,共3页
Shandong Chemical Industry
关键词
双格氏试剂
双齿膦配体
有机合成
di - Grignard reagents
bidentate phosphine ligands
organic synthesis