摘要
用高效液相色谱法测定饲料中盐酸克伦特罗的含量。选用ShimpackCLC-ODS分析柱(46mm×150mm),流动相:甲醇:水=75:25,检测波长:243nm,流速:1ml/min。盐酸克伦特罗浓度在0.1-2.0μg/ml之间具有良好线性关系,相关系数0.9996。平均回收率为(101.2±9.75)%。该法快速、准确、重现性好。
HPLC was used to determine the contents of Clenbuterol Hydrochloride in feed. TheHPLC system consisted of Shimpack CLC - ODS column (4. 6mm×150mm), methanol: water(75: 25 )mixture as mobile phase, with deteetion at 243nm, flow rate 1.0ml/min. There is a good linear relationship within the range of 0. 1 - 2. 0μg/ml (r = 0. 9996), The average recovery was(101. 2± 9. 75 ) %.The methed is rapid accurate and reproducible.
出处
《兽药与饲料添加剂》
1999年第6期10-11,共2页
Veterinary Pharmaceuticals & Feed Additives