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纳米金属酞菁MPc(M=Fe,Co,Ni,Cu和Zn)的合成与表征 被引量：2

Preparation and characterization of nanoscle metal phthalocyanines MPc(M=Fe,Co,Ni,Cu,Zn)
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摘要 采用溶剂热方法以邻苯二甲腈为原料、乙二醇为溶剂在反应釜中合成了各种形貌的Fe,Co,Ni,Cu和Zn纳米金属酞菁化合物,并对它们进行了电子扫描电镜、XRD、红外光谱及紫外-可见光谱表征.结果表明,产品纯度高,产率大,形貌独特. Fe,Co,Ni,Cu,Zn＇s phthalocyanine compound nanostructure has been successfully obtained by a facile ethylene glycol solvent-thermal synthetic route.It was characterized by SEM,XRD,IR,and UV-vis spectrum.It was indicated that the obtained metal phthalocyanines with high yields and purity had the unipue morphology and structure.
作者 宁波 郭增彩 柯福波 王井峰 邵长路
机构地区 长春职业技术学院食品与生物技术分院 东北师范大学化学学院
出处 《东北师大学报（自然科学版）》 CAS CSCD 北大核心 2011年第3期80-83,共4页 Journal of Northeast Normal University(Natural Science Edition)
基金 国家自然科学基金资助项目(50572014 50972027)
关键词 金属酞菁 溶剂热 纳米 合成 表征 metal phthalocyanines solvent-thermal nano synthetize characterization
分类号 O614 [理学—无机化学]
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参考文献12

  • 1COCK M J ,COOKE G,JAFARI-FINI A. A liquid crystalline terathiafulalenyl phthalocyanines[J]. Chem Commun, 1996,16: 1925-1926.
  • 2LUO Y, GAO J, CHENG C, et al. Fabrication micro-tube of substituted Zn-phthalocyanine in large scale by simple solvent evaporation method and its surface photovoltaic properties[J]. Organic Electronics,2008,9:466-472.
  • 3COREY E J, TRAMONTANO A. Total synthesis of the quinonoid alcohol dehydrogenase eoenzyme (1) of methylotrophic bacteria[J]. J Am CHem Soc, 1981,103,5599-5600.
  • 4LEVER A B, PHEMPTEAD M R, LEZNOFF C C, et al. Recent stuties in phthalocyanine ehemistry[J].Pure Appl Chem, 1986,58 :1467-1476.
  • 5杨树卿.双核酞菁钴磺酸盐催化剂的合成方法:中国,1045414A[P],1990-05-20.
  • 6CHEN R Y,CHEN Z,ZHENG X,et al. Preparation and characterization of mSA/mCS bipolar membranes modified by CuTsPc and CuTAPc[J]. Journal of Membrane Science, 2010,355: 1-6.
  • 7余宏宇,陈发普,姜华,刘冰,李东方.四种单一磺化度锌酞菁光敏杀瘤的效应及其机理[J].第二军医大学学报,1996,17(2):120-120. 被引量：5
  • 8DOLGOS M,PANDIAN R,WOODWARD P,et al. Crystallography of novel metallophthalocyanines[J]. Chem Mater, 1996(8) : 1061-1066.
  • 9ZHANG M Y,SHAO C L,GUO Z C,et al. Hierarchical nanostructures of copper(1D phthalocyanine on electrospun TiO2 nanofibers: controllable solvothermal-fabrication and enhanced visible photocatalytic properties[J]. ACS Appl Mater Interfaces, 2011(3) :369-377.
  • 10SEOUDI R, EI-BAHY G S, El SAYED Z A. FTIR, TGA and DC electrical conductivity studies of phthaloeyanine and its complexes[J]. J Mol Struct, 2005,753: 119-126.

共引文献4

同被引文献18

  • 1法焕宝,王杏乔.卟啉及过渡金属卟啉的电化学性质[J].吉林大学学报（理学版）,2007,45(1):107-110. 被引量：10
  • 2单凝,郑文琦,法焕宝,王杏乔.5-(对-羟基苯基)-10,15,20-三苯基卟啉的金属化及性质表征[J].吉林大学学报（理学版）,2007,45(2):283-287. 被引量：5
  • 3WANG Dong,SU Lian-jiang,CHENG Xiu-li,SUN Er-jun,SHI Tong-shun.Synthesis and Purification of Porphyrin-Schiff Base Using Ethyl Vanillin[J].Chemical Research in Chinese Universities,2007,23(2):135-137. 被引量：11
  • 4FU XIAO QI,BEI FENG LI,WANG XIN,et al.Two-dimensional monolayers of single-crystallineα-Fe2O3nanospheres:preparation,characterization and SERS effect[J].Materials Letters,2009,63:185-187.
  • 5SUN LING NA,CAO MIN HUA,HU CHANG WEN.Synthesis and magnetic properties of hollowα-Fe2O3nanospherestemplated by carbon nanospheres[J].Solid State Sciences,2010,12:2020-2023.
  • 6NORIHITO KIJIMA,MASASHI YOSHINAGA,JUNJI AWAKA,et al.Microwave synthesis,characterization,and electrochemicalproperties ofα-Fe2O3nanoparticles[J].Solid State Ionics,2011,192:293-297.
  • 7AHSANULHAQ QURASHI,ZHONG ZHONGHAI,MIR WAKAS ALAM.Synthesis and photocatalytic properties ofα-Fe2O3nanoellipsoids[J].Solid State Sciences,2010,12:1516-1519.
  • 8SEIICHI TAKAMI,TERUYUKI SATO,TAHEREH MOUSAVAND,et al.Hydrothermal synthesis of surface-modified ironoxide nanoparticles[J].Materials Letters,2007,61:4769-4772.
  • 9SREEJA V,JOY P A.Microwave-hydrothermal synthesis ofγ-Fe2O3nanoparticles and their magnetic properties[J].MaterialsResearch Bulletin,2007,42:1570-1576.
  • 10CHEN D,XU R.Hydrothermal synthesis and characterization of nanocrystalline Fe3O4powders[J].Materials ResearchBulletin,1998,33:1015-1021.

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东北师大学报（自然科学版）
2011年 第3期

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